呋喃并[3,2-b]吡啶4-氧化物合成路线 (共 8 条)
反应条件
3-chloro-benzenecarboperoxoic acid in dichloromethane 20 h; Ambient temperature;
参考文献
Shiotani, Shunsaku; Taniguchi, Katsunori
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 4 p. 1051 - 1056
反应条件
1: 45 percent / triethylamine, benzoyl chloride / CH2Cl2 / 20 h / Ambient temperature 2: 78 percent / sodium ethoxide / 5 h / Ambient temperature 3: 97 percent / 10percent hydrochloric acid / ethanol; H2O / 14 h / Ambient temperature View Scheme
参考文献
Shiotani, Shunsaku; Taniguchi, Katsunori
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 4 p. 1051 - 1056
反应条件
trichlorophosphate in chloroform 2 h; Heating / reflux;
参考文献
ARRAY BIOPHARMA INC.
Patent: WO2005/51304 A2, 2005 ;
Location in patent: Page/Page column 144-145 ;
WO 2005/051304 A2
反应条件
trichlorophosphate in chloroform 1.5 h; Heating;
参考文献
Shiotani, Shunsaku; Taniguchi, Katsunori
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 4 p. 1051 - 1056
反应条件
triethylamine in acetonitrile T=100 - 110°C; 18 h;
参考文献
Shiotani, Shunsaku; Taniguchi, Katsunori
Journal of Heterocyclic Chemistry, 1997 , vol. 34, # 2 p. 493 - 499
反应条件
benzoyl chloride in dichloromethane; water 48 h; Ambient temperature;
参考文献
Shiotani, Shunsaku; Taniguchi, Katsunori
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 4 p. 1051 - 1056
反应条件
benzoyl chloride; triethylamine in dichloromethane 20 h; Ambient temperature;
参考文献
Shiotani, Shunsaku; Taniguchi, Katsunori
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 4 p. 1051 - 1056
反应条件
1: 45 percent / triethylamine, benzoyl chloride / CH2Cl2 / 20 h / Ambient temperature
2: 71 percent / KOH / aq. ethanol / 2 h / Heating
View Scheme
参考文献
Shiotani, Shunsaku; Taniguchi, Katsunori
Journal of Heterocyclic Chemistry, 1996 , vol. 33, # 4 p. 1051 - 1056