2,5-二甲基苯基(4-甲基苯基)砜合成路线 （共 9 条）
反应条件
silica gel-supported aluminum chloride T=80°C; 1.5 h; Neat (no solvent);
参考文献
Parvanak Boroujeni, Kaveh
Journal of Sulfur Chemistry, 2010 , vol. 31, # 3 p. 197 - 203
反应条件
tin(II) trifluoromethanesulfonate T=120°C; Friedel-Crafts sulfonylation; 8 h;
参考文献
Singh, Ravi P; Kamble, Rajesh M; Chandra, Kusum L; Saravanan; Singh, Vinod K
Tetrahedron, 2001 , vol. 57, # 1 p. 241 - 247
反应条件
trifluoromethylsulfonic anhydride in tetrachloroethane, 1,1,2,2- T=80°C; 12 h;
参考文献
Yao, Bangben; Zhang, Yuhong
Tetrahedron Letters, 2008 , vol. 49, # 37 p. 5385 - 5388
反应条件
1: NMPTsO With TPPD in dichloromethane 0.5 h; 2: para-xylene in dichloromethane T=0 - 20°C; 1 h; chemoselective reaction;
参考文献
Khodaei; Nazari
Journal of the Iranian Chemical Society, 2012 , vol. 9, # 4 p. 507 - 512
反应条件
Fe(3+)-montmorillonite T=120°C; Substitution; Friedel-Crafts sulfonylation; 6 h;
参考文献
Choudary, Boyapati M.; Chowdari, N. Sreenivasa; Kantam, M. Lakshmi
Journal of the Chemical Society, Perkin Transactions 1, 2000 , # 16 p. 2689 - 2693
反应条件
trifluoromethylsulfonic anhydride in tetrachloroethane, 1,1,2,2- T=120°C; 12 h; Product distribution; Further Variations:ReagentsSolventsTemperatures;
参考文献
Yao, Bangben; Zhang, Yuhong
Tetrahedron Letters, 2008 , vol. 49, # 37 p. 5385 - 5388
反应条件
1.1: neat (no solvent) / 20 °C 2.1: TPPD / dichloromethane / 0.5 h 2.2: 1 h / 0 - 20 °C View Scheme
参考文献
Khodaei; Nazari
Journal of the Iranian Chemical Society, 2012 , vol. 9, # 4 p. 507 - 512
反应条件
aluminium trichloride
参考文献
Kraft; Urezkaja
Zhurnal Organicheskoi Khimii, 1965 , vol. 1, p. 696; engl. Ausg. S. 697
反应条件
(i) CF3SO3Ag, (ii) /BRN= 1901563/; Multistep reaction;
参考文献
Effenberger,F.; Huthmacher,K.
Chemische Berichte, 1976 , vol. 109, p. 2315 - 2326
