反应条件
1: 93 percent / imidazole / CH2Cl2; dimethylformamide / 1.) RT, 15 h, 2.) 45 deg C, 20 h, 3.) 80 deg C, 6 h 2: 1.) ozone, 2.) NaBH4 / 1.) MeOH, pyridine, CH2Cl2, -78 deg C, 1 h, 2.) RT, 12 h 3: 95 percent / pyridine / 2 h / 0 °C View Scheme
参考文献
Mascarenas, J. L.; Mourino, A.; Castedo, L.
Journal of Organic Chemistry, 1986 , vol. 51, # 8 p. 1269 - 1272
