2-甲基-2-丙基4-{[(苄氧基)羰基][5-(苄氧基)-5-氧代戊基]氨基}-1-哌啶羧酸酯合成路线 （共 6 条）
反应条件
sodium hydrogencarbonate in water; ethyl acetate T=25°C; 4 h;
参考文献
Tetrahedron Letters, , vol. 37, # 35 p. 6327 - 6330
反应条件
1: 67 percent / NaBH(OAc)3 / acetic acid; CH2Cl2 / 3 h / 25 °C 2: 100 percent / NaHCO3 / ethyl acetate; H2O / 4 h / 25 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 35 p. 6327 - 6330
反应条件
1: 67 percent / NaBH(OAc)3 / acetic acid; CH2Cl2 / 3 h / 25 °C 2: 100 percent / NaHCO3 / ethyl acetate; H2O / 4 h / 25 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 35 p. 6327 - 6330
反应条件
1: 83 percent / tosylchloride / 2.5 h / 80 °C 2: 67 percent / NaBH(OAc)3 / acetic acid; CH2Cl2 / 3 h / 25 °C 3: 100 percent / NaHCO3 / ethyl acetate; H2O / 4 h / 25 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 35 p. 6327 - 6330
反应条件
1: 83 percent / tosylchloride / 2.5 h / 80 °C 2: 67 percent / NaBH(OAc)3 / acetic acid; CH2Cl2 / 3 h / 25 °C 3: 100 percent / NaHCO3 / ethyl acetate; H2O / 4 h / 25 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 35 p. 6327 - 6330
反应条件
1: 83 percent / tosylchloride / 2.5 h / 80 °C 2: 67 percent / NaBH(OAc)3 / acetic acid; CH2Cl2 / 3 h / 25 °C 3: 100 percent / NaHCO3 / ethyl acetate; H2O / 4 h / 25 °C View Scheme
参考文献
Tetrahedron Letters, , vol. 37, # 35 p. 6327 - 6330
