1-碘-2-三甲基硅基乙炔合成路线 （共 14 条）
反应条件
1: With n-butyllithium in tetrahydrofuran T=-78°C; 2: With iodine
参考文献
Camps, Pelayo; Gomez, Tania
Arkivoc, 2011 , vol. 2011, # 3 p. 128 - 139
反应条件
iodine cloride in tetrachloromethane Ambient temperature;
参考文献
Al-Hassan, Mohammed I.
Journal of Organometallic Chemistry, 1989 , vol. 372, p. 183 - 186
反应条件
Yield given. Multistep reaction;
参考文献
Tetrahedron, , vol. 36, # 82 p. 1215 - 1222
参考文献
Oliver,R.; Walton,D.R.M.
Tetrahedron Letters, 1972 , p. 5209 - 5212
反应条件
1: 2-oxo-2H-pyran-5-carboxylic acid methyl ester; 1-iodo-2-trimethylsilylethyne in 1,2-dichloro-benzene 24 h; Reflux; 2: furan With silver fluoride; cesium fluoride in acetonitrile 6 h; Reflux;
参考文献
Crossley, James A.; Kirkham, James D.; Browne, Duncan L.; Harrity, Joseph P. A.
Tetrahedron Letters, 2010 , vol. 51, # 50 p. 6608 - 6610
反应条件
1: in 1,2-dichloro-benzene 24 h; Reflux; 2: With furan; silver fluoride in acetonitrile 6 h; Reflux;
参考文献
Crossley, James A.; Kirkham, James D.; Browne, Duncan L.; Harrity, Joseph P. A.
Tetrahedron Letters, 2010 , vol. 51, # 50 p. 6608 - 6610
反应条件
1: 2-oxo-2H-pyran-5-carboxylic acid methyl ester; 1-iodo-2-trimethylsilylethyne in 1,2-dichloro-benzene 24 h; Reflux; 2: furan With silver fluoride; cesium fluoride in acetonitrile 6 h; Reflux;
参考文献
Crossley, James A.; Kirkham, James D.; Browne, Duncan L.; Harrity, Joseph P. A.
Tetrahedron Letters, 2010 , vol. 51, # 50 p. 6608 - 6610
反应条件
1: in 1,2-dichloro-benzene 24 h; Reflux; 2: With furan; silver fluoride in acetonitrile 6 h; Reflux;
参考文献
Crossley, James A.; Kirkham, James D.; Browne, Duncan L.; Harrity, Joseph P. A.
Tetrahedron Letters, 2010 , vol. 51, # 50 p. 6608 - 6610
参考文献
Tetrahedron Letters, , p. 5209 - 5212
反应条件
n-butyllithium; copper(I) bromide
Yield given. Multistep reaction;
参考文献
Ruitenberg, K.; Meijer, J.; Bullee, R. J.; Vermeer, P.
Journal of Organometallic Chemistry, 1981 , vol. 217, # 2 p. 267 - 271
