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结构式
乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
伐地考昔杂质D
合成路线
（共 5 条）
37928-17-9
5-甲基-3,4-二苯基-异噁唑
→
反应条件
181696-35-5
伐地考昔杂质D
反应条件
sulfuric acid; sulfur trioxide T=5 - 25°C; 1.33333 h;
参考文献
Reddy, Anumula Raghupathi; Goverdhan, Gilla; Sampath, Aalla; Mukkanti, Khagga; Reddy, Padi Pratap; Bandichhor, Rakeshwar
Synthetic Communications, 2012 , vol. 42, # 5 p. 639 - 649
509074-26-4
4-(5-甲基-3-苯基异噁唑-4-基)苯磺酰氯
→
反应条件
181696-35-5
伐地考昔杂质D
反应条件
water in tetrahydrofuran 24 h; Reflux;
参考文献
Reddy, Anumula Raghupathi; Goverdhan, Gilla; Sampath, Aalla; Mukkanti, Khagga; Reddy, Padi Pratap; Bandichhor, Rakeshwar
Synthetic Communications, 2012 , vol. 42, # 5 p. 639 - 649
52201-28-2
1-(1-甲基-2-苯基 乙烯)-吡咯烷
→
反应条件
181696-35-5
伐地考昔杂质D
反应条件
1: triethylamine / dichloromethane / 5 - 35 °C / Large scale reaction 2: hydrogenchloride / water / 98 - 102 °C / Large scale reaction 3: chlorosulfonic acid / dichloromethane / 0 °C / Reflux 4: water / tetrahydrofuran / 24 h / Reflux View Scheme
参考文献
Reddy, Anumula Raghupathi; Goverdhan, Gilla; Sampath, Aalla; Mukkanti, Khagga; Reddy, Padi Pratap; Bandichhor, Rakeshwar
Synthetic Communications, 2012 , vol. 42, # 5 p. 639 - 649
103-79-7
苯基丙酮
→
反应条件
181696-35-5
伐地考昔杂质D
反应条件
1: cyclohexane / 8 h / 70 - 80 °C / Large scale reaction 2: triethylamine / dichloromethane / 5 - 35 °C / Large scale reaction 3: hydrogenchloride / water / 98 - 102 °C / Large scale reaction 4: chlorosulfonic acid / dichloromethane / 0 °C / Reflux 5: water / tetrahydrofuran / 24 h / Reflux View Scheme
参考文献
Reddy, Anumula Raghupathi; Goverdhan, Gilla; Sampath, Aalla; Mukkanti, Khagga; Reddy, Padi Pratap; Bandichhor, Rakeshwar
Synthetic Communications, 2012 , vol. 42, # 5 p. 639 - 649
857259-65-5
→
反应条件
181696-35-5
伐地考昔杂质D
反应条件
1: hydrogenchloride / water / 98 - 102 °C / Large scale reaction 2: chlorosulfonic acid / dichloromethane / 0 °C / Reflux 3: water / tetrahydrofuran / 24 h / Reflux View Scheme
参考文献
Reddy, Anumula Raghupathi; Goverdhan, Gilla; Sampath, Aalla; Mukkanti, Khagga; Reddy, Padi Pratap; Bandichhor, Rakeshwar
Synthetic Communications, 2012 , vol. 42, # 5 p. 639 - 649
