3,6-二氯-2-(三氯甲基)吡啶合成路线 (共 5 条)
反应条件
chlorine; ZnCl2, HCl, water and type L zeolite (EZ-200) mixed, dried and calcined T=200°C; P=25.8581 Torr; 12.5 h;
参考文献
Livingston, Dana Alan; Wan, Hawk Suewah; Larson, Kenneth Michael; Schoeman, Brian John
Patent: US2004/176607 A1, 2004 ;
Location in patent: Page 3-4 ;
反应条件
1: With chlorine T=195°C; 36 h; Industry scale; 2: With chlorine T=170°C; 8 h; UV-irradiationIndustry scale; Product distribution / selectivity;
参考文献
Dai, Feng
Patent: US2010/65416 A1, 2010 ;
Location in patent: Page/Page column 5 ;
反应条件
chlorine T=245°C; Irradiation;
参考文献
Emel'yanov, V. I.; Stul', B. Ya.; Korolev, B. M.
Journal of Organic Chemistry USSR (English Translation), 1983 , vol. 19, # 6 p. 1168 - 1171
Zhurnal Organicheskoi Khimii, 1983 , vol. 19, # 6 p. 1308 - 1312
反应条件
1: With chlorine Industry scale; 2: With chlorine UV-irradiationIndustry scale; Product distribution / selectivity;
参考文献
Dai, Feng
Patent: US2010/65416 A1, 2010 ;
Location in patent: Page/Page column 5 ;
反应条件
chlorine T=185°C; 21 h; various temperatures, residence times and chlorine feed rates; Product distributionRate constant;
参考文献
Emel'yanov, V. I.; Stul',B. Ya.
J. Appl. Chem. USSR (Engl. Transl.), 1983 , vol. 56, # 11 p. 2547 - 2550,2362 - 2365