1,3-二苯基-2-丙炔-1-醇合成路线 （共 82 条）
反应条件
ammonium fluoride in dichloromethane T=-20 - 0°C; 1 h;
参考文献
Tetrahedron Letters, , vol. 46, # 41 p. 7059 - 7063
反应条件
1: With P(PhCH2NCH2CH2)3N in tetrahydrofuran T=25°C; Inert atmosphere; 2: With hydrogenchloride in tetrahydrofuran; water 1 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 74, # 17 p. 6681 - 6690
反应条件
in n-heptane T=20°C; 1 h; Inert atmosphere;
参考文献
Advanced Synthesis and Catalysis, , vol. 351, # 16 p. 2595 - 2598
反应条件
copper(l) iodide in N,N-dimethyl-formamide 6 h; Ambient temperature;
参考文献
Synthesis, , # 9 p. 1252 - 1254
反应条件
1: (phenylethynyl)magnesium chloride; methyl 2-chloro-2-(cyclopropylidene)acetate in tetrahydrofuran; diethyl ether T=0 - 20°C; Michael addition; 0.5 h; 2: benzaldehyde in tetrahydrofuran; diethyl ether T=0 - 20°C; 0.5 h;
参考文献
Synthesis, , # 3 p. 471 - 479
反应条件
C20H12O2(2-)*2K(1+) in tetrahydrofuran; hexane T=0°C;
参考文献
Tetrahedron, , vol. 66, # 39 p. 7726 - 7731
反应条件
cerium(III) chloride heptahydrate; iodine; sodium iodide in acetonitrile T=110°C; Microwave irradiation;
参考文献
European Journal of Organic Chemistry, , # 3 p. 630 - 636
反应条件
sodium nitrite in water; N,N-dimethyl-formamide 24 h; Ambient temperature; Yield given;
参考文献
Journal of Organic Chemistry, , vol. 53, # 12 p. 2870 - 2872
反应条件
hydrogenchloride; water in tetrahydrofuran 0.25 h; Inert atmosphere;
参考文献
Journal of Organic Chemistry, , vol. 74, # 7 p. 2904 - 2906
反应条件
1: phenylacetylene With n-butyllithium in tetrahydrofuran; hexane T=-30°C; 0.5 h; 2: Lithium enolate of the acetaldehyde; benzaldehyde in tetrahydrofuran; hexane T=-70 - -40°C; optical yield given as percent de;
参考文献
Chemistry - A European Journal, , vol. 14, # 30 p. 9131 - 9134
