4-苯基-3-丁炔-2-酮合成路线 (共 131 条)
反应条件
in N,N-dimethyl-formamide T=60 - 70°C; 13 h;
参考文献
Lee, Ka Young; Lee, Mi Jung; GowriSankar, Saravanan; Kim, Jae Nyoung
Tetrahedron Letters, 2004 , vol. 45, # 26 p. 5043 - 5046
反应条件
aluminium trichloride in dichloromethane 2 h; Ambient temperature;
参考文献
Kashin, A. N.; Bumagin, N. A.; Kalinovskii, I. O.; Beletskaya, I. P.; Reutov, O. A.
Journal of Organic Chemistry USSR (English Translation), 1980 , vol. 16, # 7 p. 1329 - 1334
Zhurnal Organicheskoi Khimii, 1980 , vol. 16, # 7 p. 1569 - 1575
反应条件
1: phenylacetylene With n-butyllithium in tetrahydrofuran 2: N,O-dimethylacetohydroxamic acid in tetrahydrofuran
参考文献
Organic Letters, , vol. 15, # 9 p. 2262 - 2265
反应条件
1: phenylacetylene With ethyl bromide; iodine; magnesium in tetrahydrofuran T=35°C; Large scale; 2: acetic anhydride in tetrahydrofuran T=3 - 8°C; Large scale;
参考文献
Organic Process Research and Development, , vol. 2, # 1 p. 60 - 62
反应条件
air; (R,R)-(nitroso)(salen)ruthenium(II) chloride in chlorobenzene T=20°C; resolution of racemate; oxidation; 17 h; Irradiation;
参考文献
Masutani, Kouta; Uchida, Tatsuya; Irie, Ryo; Katsuki, Tsutomu
Tetrahedron Letters, 2000 , vol. 41, # 26 p. 5119 - 5123
参考文献
Journal of the American Chemical Society, , vol. 58, p. 1862
反应条件
in 1,2-dichloro-benzene Heating;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 36, # 2 p. 613 - 620
反应条件
in n-heptane Heating;
参考文献
Gusev, B. P.; El'perina, E. A.; Kucherov, V. F.
Bulletin of the Academy of Sciences of the USSR, Division of Chemical Science (English Translation), 1980 , vol. 29, # 3 p. 418 - 420
Izvestiya Akademii Nauk SSSR, Seriya Khimicheskaya, 1980 , # 3 p. 600 - 603
反应条件
dichloro bis(acetonitrile) palladium(II) in tetrahydrofuran; N,N,N',N',N'',N''-hexamethylphosphoric triamide T=50°C; 1 h; Product distribution;
参考文献
Doklady Chemistry, , vol. 291, p. 471 - 474
Dokl. Akad. Nauk SSSR Ser. Khim., , vol. 291, # 4 p. 868 - 872
反应条件
tetrafluoroboric acid diethyl ether complex; 2-fluoro-pyridine in tetrahydrofuran; di-isopropyl ether T=97°C; 0.516667 h; other azadiyne; Product distributionMechanism;
参考文献
Journal of the American Chemical Society, , vol. 120, # 2 p. 376 - 385