triethylamine in acetonitrile T=0 - 20°C; Inert atmosphere; Reagent/catalyst;

triethylamine in acetonitrile T=0 - 20°C; Inert atmosphere; Reagent/catalyst;

phosphorus trichoride in acetonitrile T=20°C; 2 h;

1: With trifuran-2-yl-phosphane; tetra-(n-butyl)ammonium iodide; tris-(dibenzylideneacetone)dipalladium(0) in 1-methyl-pyrrolidin-2-one T=20°C; Negishi Coupling Reaction; 2: With ammonium chloride in 1-methyl-pyrrolidin-2-one; water

tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran T=50°C; Negishi coupling; 14 h;