(E)-1,2-乙烯二基二(三甲基-硅烷合成路线 （共 16 条）
反应条件
1: Br2 / CH2Cl2 2: KF / dimethylsulfoxide / 1 h / Ambient temperature 3: 16 h / 180 °C View Scheme
参考文献
Pillot,J.P. et al.
Synthetic Communications, 1979 , vol. 9, p. 395 - 406
反应条件
1: AlCl3 / CH2Cl2 / -40 °C 2: LiAlH4 View Scheme
参考文献
Pillot,J.-P. et al.
Bulletin de la Societe Chimique de France, 1975 , p. 2143 - 2146
反应条件
ozone T=20°C; ozonolysis; 0.666667 h; Product distribution;
参考文献
Fajgar, Radek; Pola, Josef
Tetrahedron Letters, 2000 , vol. 41, # 14 p. 2435 - 2438
反应条件
aluminium trichloride in dichloromethane T=-40°C;
参考文献
Pillot,J.-P. et al.
Bulletin de la Societe Chimique de France, 1975 , p. 2143 - 2146
反应条件
1: 98 percent / pentane / 20 h / -10 °C 2: 42 percent / tetrachloro-o-benzoquinone / benzene / 14 h / Ambient temperature View Scheme
参考文献
Birkofer, Leonhard; Kuehn, Thomas
Chemische Berichte, 1981 , vol. 114, # 6 p. 2293 - 2299
反应条件
palladium diacetate; triethylamine in N,N-dimethyl-formamide T=110°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Karabelas, Kostas; Hallberg, Anders
Journal of Organic Chemistry, 1989 , vol. 54, # 7 p. 1773 - 1776
反应条件
palladium diacetate; triethylamine; lithium iodide in N,N-dimethyl-formamide T=110°C; 2 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Karabelas, Kostas; Hallberg, Anders
Journal of Organic Chemistry, 1989 , vol. 54, # 7 p. 1773 - 1776
反应条件
palladium diacetate; triethylamine in N,N-dimethyl-formamide
T=110°C; 2 h; var. aryl iodides or aryl triflates/lithium halide, in presence of silver nitrate; Product distributionMechanism;
参考文献
Karabelas, Kostas; Hallberg, Anders
Journal of Organic Chemistry, 1989 , vol. 54, # 7 p. 1773 - 1776
反应条件
palladium diacetate; silver nitrate; triethylamine in dimethyl sulfoxide
T=70°C; 6 h; Yield given. Yields of byproduct given. Title compound not separated from byproducts;
参考文献
Karabelas, Kostas; Hallberg, Anders
Journal of Organic Chemistry, 1989 , vol. 54, # 7 p. 1773 - 1776
反应条件
palladium diacetate; triethylamine in N,N-dimethyl-formamide
T=110°C; 2 h; var. aryl iodides or aryl triflates/lithium halide, in presence of silver nitrate; Product distributionMechanism;
参考文献
Karabelas, Kostas; Hallberg, Anders
Journal of Organic Chemistry, 1989 , vol. 54, # 7 p. 1773 - 1776
