1,4-苯二甲酸氢1-丁酯合成路线 (共 8 条)
反应条件
potassium hydroxide in butan-1-ol 3.5 h; Heating;
参考文献
Chenot, Elodie-Denise; Bernardi, Dan; Comel, Alain; Kirsch, Gilbert
Synthetic Communications, 2007 , vol. 37, # 3 p. 483 - 490
反应条件
triethylamine 1 h; HeatingInert atmosphereIonic liquid;
参考文献
Goek, Yetkin; Alici, Buelent; Cetinkaya, Enginc; OeZdemir, Ismail; Oezeroglu, Ozlem
Turkish Journal of Chemistry, 2010 , vol. 34, # 2 p. 187 - 191
反应条件
1: 95 percent / thionyl chloride / Heating 2: 13 percent / potassium hydroxide / butan-1-ol / 3.5 h / Heating View Scheme
参考文献
Chenot, Elodie-Denise; Bernardi, Dan; Comel, Alain; Kirsch, Gilbert
Synthetic Communications, 2007 , vol. 37, # 3 p. 483 - 490
反应条件
1: KOH 2: CDI; HOBT / tetrahydrofuran 3: CF3COOH / CHCl3 / 20 °C View Scheme
参考文献
Seliger, H.; Bitar, M. B.; Goeldner, E.; Kittel, I.; Kilian, H. G.
Revue Roumaine de Chimie, 1991 , vol. 36, # 1-3 p. 171 - 186
反应条件
1: CDI; HOBT / tetrahydrofuran 2: CF3COOH / CHCl3 / 20 °C View Scheme
参考文献
Seliger, H.; Bitar, M. B.; Goeldner, E.; Kittel, I.; Kilian, H. G.
Revue Roumaine de Chimie, 1991 , vol. 36, # 1-3 p. 171 - 186
反应条件
2: KOH 3: CDI; HOBT / tetrahydrofuran 4: CF3COOH / CHCl3 / 20 °C View Scheme
参考文献
Seliger, H.; Bitar, M. B.; Goeldner, E.; Kittel, I.; Kilian, H. G.
Revue Roumaine de Chimie, 1991 , vol. 36, # 1-3 p. 171 - 186
参考文献
Du Pont de Nemours and Co.
Patent: US2479066 , 1947 ;
反应条件
hydroxylamine hydrochloride
参考文献
Hynes
Journal of medicinal chemistry, 1970 , vol. 13, # 6 p. 1235 - 1237