1,3-二甲氧基-1,1,3,3-四甲基二硅氧烷合成路线 (共 13 条)
反应条件
1: methanol With 5 palladium on charcoal in water T=50°C; Reflux; 2: 1,1,3,3-tetramethyldisiloxane T=50°C; 2.75 h; Product distribution / selectivity;
参考文献
WACKER CHEMIE AG
Patent: US2012/10422 A1, 2012 ;
Location in patent: Page/Page column 6 ;
参考文献
Sekeguchi,A.; Ando,W.
Journal of the American Chemical Society, 1984 , vol. 106, p. 1486
反应条件
1,1,1,4,4,4-hexafluoro-2-butyne T=65°C; 6 h; Yield given. Yields of byproduct given;
参考文献
Hussmann, Gregory; Wulff, William D.; Barton, Thomas J.
Journal of the American Chemical Society, 1983 , vol. 105, # 5 p. 1263 - 1269
反应条件
dimethoxy dimethyl silane T=65°C; 6 h; Yield given. Yields of byproduct given;
参考文献
Hussmann, Gregory; Wulff, William D.; Barton, Thomas J.
Journal of the American Chemical Society, 1983 , vol. 105, # 5 p. 1263 - 1269
反应条件
in tetrahydrofuran 2 h; Irradiation; Yield given. Yields of byproduct given;
参考文献
Hussmann, Gregory; Wulff, William D.; Barton, Thomas J.
Journal of the American Chemical Society, 1983 , vol. 105, # 5 p. 1263 - 1269
反应条件
(i) hexafluoro-but-2-yne, (ii) /BRN= 1733694/; Multistep reaction;
参考文献
Barton,T.J.; Wulff,W.D.
Journal of the American Chemical Society, 1979 , vol. 101, p. 2735 - 2736
反应条件
sodium hydrogencarbonate
参考文献
Tanaka; Okawara
Bulletin of the Chemical Society of Japan, 1955 , vol. 28, p. 364
反应条件
acetate buffer in water T=25°C; Rate constant;
参考文献
Lasocki, Zygmunt; Witekowa, Malgorzata
Journal of Organometallic Chemistry, 1991 , vol. 408, # 1 p. 27 - 33
反应条件
acetate buffer in water T=25°C; effect of various acetate buffer concentrations; Rate constant;
参考文献
Lasocki, Zygmunt; Witekowa, Malgorzata
Journal of Organometallic Chemistry, 1986 , vol. 311, p. 17 - 26
参考文献
Lane,T.H.; Frye,C.L.
Journal of Organometallic Chemistry, 1979 , vol. 172, p. 213 - 221