1: With sodium tetrahydroborate; zirconium tetrachloride in tetrahydrofuran T=0 - 20°C; 4 h; Inert atmosphere; 2: With hydrogenchloride in tetrahydrofuran; water Cooling with ice;
参考文献
Mistry, Shailesh N.; Baker, Jillian G.; Fischer, Peter M.; Hill, Stephen J.; Gardiner, Sheila M.; Kellam, Barrie
Journal of Medicinal Chemistry, 2013 , vol. 56, # 10 p. 3852 - 3865
lithium aluminium tetrahydride; zirconium tetrachloride in diethyl ether T=30°C; 12 h; Yields of byproduct given. Title compound not separated from byproducts;
