Nα-Fmoc-L-2,3-二氨基丙酸合成路线 (共 4 条)
反应条件
1: With bis-[(trifluoroacetoxy)iodo]benzene in water; N,N-dimethyl-formamide 0.25 h; 2: With pyridine in water; N,N-dimethyl-formamide 10 h;
参考文献
Akaji, Kenichi; Aimoto, Saburou
Tetrahedron, 2001 , vol. 57, # 9 p. 1749 - 1755
反应条件
trifluoroacetic acid in dichloromethane 1 h;
参考文献
Journal of the American Chemical Society, , vol. 124, # 38 p. 11272 - 11273
反应条件
in N,N-dimethyl-formamide T=20°C; Condensation; 24 h;
参考文献
Gopalsamy, Ariamala; Yang, Hui; Ellingboe, John W.; Kees, Kenneth L.; Yoon, Jeanne; Murrills, Richard
Bioorganic and Medicinal Chemistry Letters, 2000 , vol. 10, # 15 p. 1715 - 1718
反应条件
N-ethyl-N,N-diisopropylamine in tetrahydrofuran; N,N-dimethyl-formamide 6 h; Ambient temperature;
参考文献
Hirschmann, Ralph; Yao, Wenqing; Arison, Byron; Maechler, Laurie; Rosegay, Avery; Sprengeler, Paul A.; Smith III, Amos B.
Tetrahedron, 1998 , vol. 54, # 25 p. 7179 - 7202