1-甲基-4-(1-环己烯基)苯合成路线 （共 31 条）
反应条件
tetrakis(triphenylphosphine) palladium(0) in benzene
T=80°C; 24 h; Yield given. Yields of byproduct given;
参考文献
Kamigata, Nobumasa; Fukushima, Takamasa; Satoh, Akira; Kameyama, Masayuki
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1990 , p. 549 - 553
反应条件
1: pyridine / dichloromethane / 5 h / 25 °C / |Inert atmosphere
2: Pd(F6-acac)2; 1,3-bis-(diphenylphosphino)propane; lithium carbonate; 1,2-dimethoxy-benzene / 48 h / 120 °C / |Inert atmosphere
View Scheme
参考文献
Wu, Xiaojin; Lu, Yunpeng; Hirao, Hajime; Zhou, Jianrong
Chemistry - A European Journal, 2013 , vol. 19, # 19 p. 6014 - 6020
反应条件
1.1: magnesium; iodine / diethyl ether / 0.5 h / 0 - 20 °C / |Inert atmosphere
1.2: 20 °C / |Inert atmosphere
2.1: acetic acid / 1 h / 118 °C
View Scheme
参考文献
Rono, Lydia J.; Yayla, Hatice G.; Wang, David Y.; Armstrong, Michael F.; Knowles, Robert R.
Journal of the American Chemical Society, 2013 , vol. 135, # 47 p. 17735 - 17738
反应条件
palladium diacetate; sodium acetate in water
T=225°C; P=75006 - 150012 Torr; 0.333333 h; stainless steel reactor; Product distribution;
参考文献
Gron; Tinsley
Tetrahedron Letters, 1999 , vol. 40, # 2 p. 227 - 230
反应条件
2: phenyl isocyanate
View Scheme
参考文献
Sabatier; Mailhe
Annales de Chimie (Cachan, France), 1907 , vol. <8> 10, p. 538
参考文献
Shirakawa, Eiji; Watabe, Ryo; Murakami, Takuya; Hayashi, Tamio
Chemical Communications, 2013 , vol. 49, # 45 p. 5219 - 5221
反应条件
para-dicyanobenzene; 2,3,5-trimethyl-pyridine; biphenyl in acetonitrile
T=10°C; 2.5 h; UV-irradiation;
参考文献
Mangion, Dino; Kendall, Jamie; Arnold, Donald R.
Organic Letters, 2001 , vol. 3, # 1 p. 45 - 48
反应条件
ethanol; nickel
Hydrogenation;
参考文献
Hickinbottom; Rogers
Journal of the Chemical Society, 1957 , p. 4124,4129
反应条件
methanol; oxygen in acetonitrile
16 h; Irradiation400 W high-pressure mercury lamp; Yield given. Yields of byproduct given;
参考文献
Kojima, Masanobu; Sakuragi, Hirochika; Tokumaru, Katsumi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3331 - 3336
反应条件
oxygen in acetonitrile
16 h; Irradiation400 W high-pressure mercury lamp; Yield given. Yields of byproduct given;
参考文献
Kojima, Masanobu; Sakuragi, Hirochika; Tokumaru, Katsumi
Bulletin of the Chemical Society of Japan, 1987 , vol. 60, # 9 p. 3331 - 3336
