3,4,5-三甲氧基苯硼酸合成路线 (共 30 条)
反应条件
water T=25°C; Equilibrium constant;
参考文献
Heterocycles, , vol. 74, # C p. 219 - 223
反应条件
water T=25°C; Equilibrium constant;
参考文献
Heterocycles, , vol. 74, # C p. 219 - 223
反应条件
water T=25°C; Equilibrium constant;
参考文献
Heterocycles, , vol. 74, # C p. 219 - 223
反应条件
tris-(dibenzylideneacetone)dipalladium(0); potassium carbonate in toluene T=110°C; Suzuki-Miyaura coupling; 15 h; Inert atmosphere;
参考文献
Gerbino, Dario C.; Mandolesi, Sandra D.; Schmalz, Hans-Guenther; Podesta, Julio C.
European Journal of Organic Chemistry, 2009 , # 23 p. 3964 - 3972
反应条件
1.1: boron trifluoride diethyl etherate / dichloromethane / 0 - 20 °C 1.2: 0.5 h 2.1: Cu(OTf)2; potassium fluoride; 18-crown-6 ether / N,N-dimethyl-formamide / 18 h / 60 °C View Scheme
参考文献
Ichiishi, Naoko; Canty, Allan J.; Yates, Brian F.; Sanford, Melanie S.
Organic Letters, 2013 , vol. 15, # 19 p. 5134 - 5137
反应条件
tert.-butylhydroperoxide; copper(l) iodide in N,N-dimethyl acetamide; water T=130°C; 20 h;
参考文献
Luo, Yan; Wen, Qiaodong; Wu, Zhiyuan; Jin, Jisong; Lu, Ping; Wang, Yanguang
Tetrahedron, 2013 , vol. 69, # 39 p. 8400 - 8404
反应条件
water T=25°C; Equilibrium constant;
参考文献
Tokunaga, Yuji; Ueno, Hiroki; Shimomura, Youji
Heterocycles, 2007 , vol. 74, # C p. 219 - 223
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethylene glycol dimethyl ether Suzuki cross-coupling; Heating;
参考文献
Gaukroger, Keira; Hadfield, John A.; Hepworth, Lucy A.; Lawrence, Nicholas J.; McGown, Alan T.
Journal of Organic Chemistry, 2001 , vol. 66, # 24 p. 8135 - 8138
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium hydroxide in ethylene glycol dimethyl ether; water T=100°C; Suzuki-Miyaura cross-coupling; 0.25 h; Inert atmosphereMicrowave irradiation; optical yield given as percent destereoselective reaction;
参考文献
Bazin, Marc-Antoine; Jouanne, Marie; El-Kashef, Hussein; Rault, Sylvain
Synlett, 2009 , # 17 p. 2789 - 2794
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium chloride; sodium carbonate in ethanol; water; toluene T=100°C; Suzuki-Miyaura coupling; 3 h; Inert atmosphere;
参考文献
Organic Letters, , vol. 11, # 8 p. 1801 - 1804