3,4,5-三甲氧基苯硼酸合成路线 （共 30 条）
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile
T=140°C; Suzuki cross-coupling reaction; 0.0833333 h; microwave irradiation;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in acetonitrile
T=140°C; Suzuki cross-coupling reaction; 0.0833333 h; microwave irradiation;
参考文献
Wang, Hong-Jun; Keilman, Jeffrey; Pabba, Chittari; Chen, Zhen-Jia; Gregg, Brian T.
Tetrahedron Letters, 2005 , vol. 46, # 15 p. 2631 - 2634
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethylene glycol dimethyl ether
T=80°C; Suzuki coupling;
参考文献
Miyazaki, Yasushi; Nakano, Masato; Sato, Hideyuki; Truesdale, Anne T.; Stuart, J. Darren; Nartey, Eldridge N.; Hightower, Kendra E.; Kane-Carson, Laurie
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 1 p. 250 - 254
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in tetrahydrofuran; toluene
T=90°C;
参考文献
Kowa Co., Ltd.
Patent: EP1568691 A1, 2005 ;
Location in patent: Page/Page column 14 ;
参考文献
Kowa Co., Ltd.
Patent: US6498169 B1, 2002 ;
反应条件
tetra-butylammonium acetate; Pd EnCat-30TM in ethanol
T=120°C; Suzuki cross-coupling; 0.166667 h; microwave irradiation;
参考文献
Baxendale, Ian R.; Griffiths-Jones, Charlotte M.; Ley, Steven V.; Tranmer, Geoffrey K.
Chemistry - A European Journal, 2006 , vol. 12, # 16 p. 4407 - 4416
反应条件
Wilkinson's catalyst; 2,2,6,6-tetramethyl-1-piperidinyloxy, free radical in 1,4-dioxane; water
T=130°C; 2 h; Inert atmosphere;
参考文献
Vogler, Thomas; Studer, Armido
Advanced Synthesis and Catalysis, 2008 , vol. 350, # 13 p. 1963 - 1967
反应条件
tetrakis(triphenylphosphine) palladium(0); sodium carbonate in ethylene glycol dimethyl ether
Suzuki cross-coupling; Heating;
参考文献
Gaukroger, Keira; Hadfield, John A.; Hepworth, Lucy A.; Lawrence, Nicholas J.; McGown, Alan T.
Journal of Organic Chemistry, 2001 , vol. 66, # 24 p. 8135 - 8138
反应条件
tetrakis(triphenylphosphine) palladium(0); potassium chloride; sodium carbonate in ethanol; water; toluene
T=100°C; Suzuki-Miyaura coupling; 3 h; Inert atmosphere;
参考文献
Beaumard, Floriane; Dauban, Philippe; Dodd, Robert H.
Organic Letters, 2009 , vol. 11, # 8 p. 1801 - 1804
反应条件
sodium carbonate; tetrakis(triphenylphosphine) palladium(0) in ethanol; water; toluene
10 h; Reflux;
参考文献
FUZIANS BIOMEDICALS, INC.; THE UAB RESEARCH FOUNDATION; WANG, Guoxin; LUO, Ming; YANG, Zhen
Patent: WO2011/160024 A2, 2011 ;
Location in patent: Page/Page column 34 ;
