1-(4-甲氧基[1,1-联苯]-3-基)乙酮合成路线 （共 7 条）
反应条件
sodium carbonate; palladium on activated charcoal in ethanol; water T=20°C; Suzuki-Miyaura cross-coupling; 24 h;
参考文献
Kitamura, Yoshiaki; Sakurai, Ai; Udzu, Takahiro; Maegawa, Tomohiro; Monguchi, Yasunari; Sajiki, Hironao
Tetrahedron, 2007 , vol. 63, # 43 p. 10596 - 10602
反应条件
tripotassium phosphate monohydrate; 1-methyl-2-(2-(dicyclohexylphosphino)phenyl)-1H-benzoimidazole; palladium diacetate in 1,4-dioxane; 1,3,5-trimethyl-benzene T=135°C; Suzuki-Miyaura coupling; 24 h; Inert atmosphere;
参考文献
Wong, Shun Man; So, Chau Ming; Chung, Kin Ho; Lau, Chak Po; Kwong, Fuk Yee
European Journal of Organic Chemistry, 2012 , # 22 p. 4172 - 4177
反应条件
tetrabutylammomium bromide; caesium carbonate; triphenylphosphine; palladium dichloride in N,N-dimethyl acetamide T=90°C; 1 h;
参考文献
Rao, Maddali L.N.; Jadhav, Deepak N.; Banerjee, Debasis
Tetrahedron, 2008 , vol. 64, # 24 p. 5762 - 5772
反应条件
8C33H27N9O3*6Pd(2+)*12NO3(1-); potassium carbonate in ethanol; water T=60°C; Suzuki-Miyaura Coupling; 10 h; Green chemistry;
参考文献
Zhao, Chao-Wei; Ma, Jian-Ping; Liu, Qi-Kui; Yu, Yang; Wang, Peng; Li, Yan-An; Wang, Kui; Dong, Yu-Bin
Green Chemistry, 2013 , vol. 15, # 11 p. 3150 - 3154
反应条件
potassium fluoride; {palladium-dichloro-(P(C3H7)3)2} in N,N-dimethyl-formamide T=120°C;
参考文献
Gouda, Ken-Ichi; Hagiwara, Emiko; Hatanaka, Yasuo; Hiyama, Tamejiro
Journal of Organic Chemistry, 1996 , vol. 61, # 21 p. 7232 - 7233
反应条件
palladium diacetate; potassium carbonate in tetrahydrofuran; water Suzuki-Miyaura coupling; 9 h; Inert atmosphereReflux;
参考文献
Razler, Thomas M.; Hsiao, Yi; Qian, Feng; Fu, Ruiling; Khan, Rana Kashif; Doubleday, Wendel
Journal of Organic Chemistry, 2009 , vol. 74, # 3 p. 1381 - 1384
反应条件
in hydrogen bromide; acetic acid
参考文献
Astra Pharmaeuticals Ltd.
Patent: US5977105 A1, 1999 ;
US 5977105 A
