2-(4-甲氧苯基)-氯乙烷合成路线 (共 30 条)
反应条件
thionyl chloride in benzene T=50°C; 2 h;
参考文献
Kato; Takemoto; Achiwa
Chemical and Pharmaceutical Bulletin, 1993 , vol. 41, # 11 p. 2003 - 2006
反应条件
1: 85 percent / lithium aluminum hydride / diethyl ether / 0.5 h / Heating 2: 75 percent / thionyl chloride / benzene / 2 h / 50 °C View Scheme
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 41, # 11 p. 2003 - 2006
反应条件
N-chloro-succinimide in tetrahydrofuran 16 h; Ambient temperatureIrradiation;
参考文献
Collazo, Luis R.; Guziec, Frank S.; Hu, Wei-Xiao Jr.; Pankayatselvan, Ratnadevi
Tetrahedron Letters, 1994 , vol. 35, # 43 p. 7911 - 7914
反应条件
Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 57, # 14 p. 3772 - 3776
反应条件
2: 1.) base, 2.) O-(2,4-dinitrophenyl)hydroxylamine 3: 82 percent / NCS / tetrahydrofuran / 16 h / Ambient temperature; Irradiation View Scheme
参考文献
Tetrahedron Letters, , vol. 35, # 43 p. 7911 - 7914
反应条件
tetraethylammonium chloride in acetonitrile Heating;
参考文献
Bulletin of the Chemical Society of Japan, , vol. 44, # 11 p. 3091 - 3095
反应条件
potassium hydroxide; cis amino chloride 1.) ether, 0 deg C, 2.) MeOH, reflux; Yield given. Multistep reaction;
参考文献
Journal of Organic Chemistry, , vol. 57, # 14 p. 3772 - 3776
反应条件
1: diethyl ether; benzene 2: pyridine; SOCl2 View Scheme
参考文献
Journal of the Chemical Society, , p. 694,697
参考文献
Journal of Applied Chemistry, , vol. 1, p. 95