4-氯-5-苯基噻酚[2,3-D]嘧啶合成路线 (共 2 条)
反应条件
thionyl chloride; N,N-dimethyl-formamide T=80°C; 4 h; Product distribution / selectivity;
参考文献
4SC AG
Patent: EP1947103 A1, 2008 ;
Location in patent: Page/Page column 18 ;
EP 1947103 A1
反应条件
1: 63 percent / 4 h / Heating 2: 74 percent / PCl5, POCl3 / 3 h / Heating View Scheme
参考文献
Synthetic Communications, , vol. 26, # 20 p. 3733 - 3755