反应条件
1: 84 percent / PdCl2(PPh3)2, Bu3SnH, HOAc / CH2Cl2 / 0.08 h / 23 °C 2: 70 percent / <N-methylpyridinium-4-carboxaldehyde>iodide, 1,8-diazabicyclo<6.4.0>undec-7-ene, DMF / CH2Cl2 / 0.67 h / 23 °C 3: 82 percent / silica gel / ethanol / 23 °C 4: aq. CF3COOH / tetrahydrofuran / 9 h / 23 °C 5: aq. AgNO3 / acetonitrile / 11 h / 23 °C View Scheme
参考文献
Corey; Gin, David Y.; Kania, Robert S.
Journal of the American Chemical Society, 1996 , vol. 118, # 38 p. 9202 - 9203