1,3,5-三(溴甲基)苯合成路线 （共 27 条）
反应条件
N-bromosuccinmide; dibenzoyl peroxide in tetrachloromethane T=70°C; 12 h;
参考文献
Wang, Liang; Yi, Wen-Bin; Cai, Chun
Chemical Communications, 2011 , vol. 47, # 2 p. 806 - 808
反应条件
hydrogen bromide in acetic acid T=20°C; 46 h;
参考文献
Ashton, Peter R.; Shibata, Kazusato; Shipway, Andrew N.; Stoddart, J. Fraser
Angewandte Chemie, International Edition in English, 1997 , vol. 36, # 24 p. 2781 - 2783
Angewandte Chemie, 1997 , vol. 109, p. 2902 - 2905
反应条件
N-bromosuccinmide; 2,2'-azo-bisisobutyronitrile in cyclohexane 0.5 h; Heating / reflux; Product distribution / selectivity;
参考文献
HELM AG
Patent: US2006/217569 A1, 2006 ;
Location in patent: Page/Page column 3; 4 ;
反应条件
N-bromosuccinmide; dibenzoyl peroxide in benzene T=85°C; 12 h;
参考文献
Lee, Insuk; You, Ngmin; Lim, Seon-Jeong; Park, Soo Young
Chemistry Letters, 2007 , vol. 36, # 7 p. 888 - 889
反应条件
lithium aluminium tetrahydride; hydrogen bromide 1.) THF, reflux, 16 h, 2.) benzene, reflux, 16 h; Yield given. Multistep reaction;
参考文献
Canadian Journal of Chemistry, , vol. 75, # 8 p. 1047 - 1054
反应条件
1: LiAlH4 / tetrahydrofuran / 24 h / Heating 2: 19.12 g / aq. HBr / toluene / 24 h / Heating View Scheme
参考文献
Journal of the American Chemical Society, , vol. 126, # 39 p. 12395 - 12402
反应条件
chloro-trimethyl-silane in butan-1-ol; benzene T=80°C; 16 h; Inert atmosphere; regioselective reaction;
参考文献
Cheng, Jinsheng; Tang, Longhua; Li, Jinghong
Journal of Nanoscience and Nanotechnology, 2011 , vol. 11, # 6 p. 5159 - 5168
反应条件
carbon tetrabromide; triphenylphosphine in tetrahydrofuran T=20°C; 2.5 h;
参考文献
Journal of Medicinal Chemistry, , vol. 55, # 23 p. 10405 - 10413
反应条件
1: LiAlH4 2: 71 percent / PBr3 / CHCl3 View Scheme
参考文献
Canadian Journal of Chemistry, , vol. 68, # 3 p. 440 - 445
反应条件
phosphorus tribromide in chloroform 2 h; Ambient temperature;
参考文献
Kadei, Klaus; Moors, Rolf; Voegtle, Fritz
Chemische Berichte, 1994 , vol. 127, # 5 p. 897 - 904
