1: 1-bromo-octane With magnesium in tetrahydrofuran
T=-78°C;
2: With copper(I) bromide; lithium bromide in tetrahydrofuran
T=-100 - -75°C;
3: oxalyl dichloride in tetrahydrofuran
T=-95 - -90°C; 1 h; Further stages.;
参考文献
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Parkinson, Elizabeth I.; Jason Hatfield; Tsurkan, Lyudmila; Hyatt, Janice L.; Edwards, Carol C.; Hicks, Latorya D.; Yan, Bing; Potter, Philip M.
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