1,1-二乙氧基己-3-炔合成路线 （共 7 条）
反应条件
N,N,N',N',N'',N''-hexamethylphosphoric triamide; n-butyllithium; calcium carbonate in tetrahydrofuran; hexane T=-78 - 20°C; Alkylation; 66 h;
参考文献
Sha, Wei; Salomon, Robert G.
Journal of Organic Chemistry, 2000 , vol. 65, # 17 p. 5315 - 5326
反应条件
camphor-10-sulfonic acid in dichloromethane T=20°C;
参考文献
Wavarin, Laurence; Viala, Jacques
Synthesis, 2002 , # 3 p. 326 - 330
反应条件
potassium tert-butylate in dimethyl sulfoxide
参考文献
Mantione,R. et al.
Bulletin de la Societe Chimique de France, 1967 , p. 2912 - 2918
反应条件
1: (i) EtMgBr, (ii) /BRN= 605384/ 2: KOtBu / dimethylsulfoxide View Scheme
参考文献
Mantione,R. et al.
Bulletin de la Societe Chimique de France, 1967 , p. 2912 - 2918
反应条件
1: (i) EtMgBr, (ii) /BRN= 605384/ 2: KOtBu / dimethylsulfoxide View Scheme
参考文献
Mantione,R. et al.
Bulletin de la Societe Chimique de France, 1967 , p. 2912 - 2918
反应条件
bis(cyclopentadienyl)titanium dichloride; 2-methylpropylmagnesium bromide in diethyl ether T=20°C; Reduction; 48 h;
参考文献
Sha, Wei; Salomon, Robert G.
Journal of Organic Chemistry, 2000 , vol. 65, # 17 p. 5315 - 5326
反应条件
1: 82 percent / i-BuMgBr; Cp2TiCl2 / diethyl ether / 48 h / 20 °C 2: 2,5-di-tert-butylhydroquinone / H2O; acetic acid / 1 h / 20 °C View Scheme
参考文献
Sha, Wei; Salomon, Robert G.
Journal of Organic Chemistry, 2000 , vol. 65, # 17 p. 5315 - 5326
