AlCl3 in neat (no solvent)
byproducts: CH3SiCl3; heated for 1 h to 125°C; stirred for 2 h; heated to 135-140°C and then at 145-150°C for 2 h; AlCl3 sepd.; vacuum-distd.; elem. anal.;
参考文献
Motsarev, G. V.; Chernyshev, E. A.; Rozenberg, V. R.; Inshakova, V. T.; Zetkin, V. I.
Journal of General Chemistry USSR (English Translation), 1983 , vol. 53, p. 985 - 988
Zhurnal Obshchei Khimii, 1988 , vol. 53, p. 1111 - 1114
