2-(3-环己烯基)乙醇合成路线 （共 20 条）
反应条件
1: 100 percent / DIBAL / hexane / a) -78 deg C, 30 min, b) 3 h
2: 44 percent / 4 A molecular sieves / benzene
3: 12 percent / n-Bu3SnH, AIBN / benzene / 30 h / Heating
View Scheme
参考文献
Yadav, Veejendra; Fallis, Alex G.
Canadian Journal of Chemistry, 1991 , vol. 69, # 5 p. 779 - 789
反应条件
1: (i) TsCl, Py, (ii) /BRN= 3587243/
2: aq. NaOH
3: SOCl2
4: (i) SnCl4, (ii) LiAlH4
View Scheme
参考文献
Monti,S.A.; White,G.L.
Journal of Organic Chemistry, 1975 , vol. 40, # 2 p. 215 - 217
反应条件
1: LiAlH4
2: (i) TsCl, Py, (ii) /BRN= 3587243/
3: aq. NaOH
4: SOCl2
5: (i) SnCl4, (ii) LiAlH4
View Scheme
参考文献
Monti,S.A.; White,G.L.
Journal of Organic Chemistry, 1975 , vol. 40, # 2 p. 215 - 217
反应条件
1: aq. NaOH
2: SOCl2
3: (i) SnCl4, (ii) LiAlH4
View Scheme
参考文献
Monti,S.A.; White,G.L.
Journal of Organic Chemistry, 1975 , vol. 40, # 2 p. 215 - 217
反应条件
1: SOCl2
2: (i) SnCl4, (ii) LiAlH4
View Scheme
参考文献
Monti,S.A.; White,G.L.
Journal of Organic Chemistry, 1975 , vol. 40, # 2 p. 215 - 217
反应条件
hydroxide; dihydrogen peroxide
参考文献
Koester,R. et al.
Justus Liebigs Annalen der Chemie, 1964 , vol. 672, p. 1 - 34
反应条件
(i) SnCl4, (ii) LiAlH4; Multistep reaction;
参考文献
Monti,S.A.; White,G.L.
Journal of Organic Chemistry, 1975 , vol. 40, # 2 p. 215 - 217
反应条件
(i) LiNEt2, HMPT, benzene, (ii) K, HMPT, tBuOH, (iii) TsOH; Multistep reaction;
参考文献
Debal,A. et al.
Synthesis, 1976 , p. 391 - 393
反应条件
pyridinium chlorochromate in dichloromethane
T=25°C; 1 h;
参考文献
Oppolzer, W.; Siles, S.; Snowden, R. L.; Bakker, B. H.; Petrzilka, M.
Tetrahedron, 1985 , vol. 41, # 17 p. 3497 - 3509
反应条件
1: pyridine / 18 h
2: NaBr, HMPA / acetone / 6 h / Heating
View Scheme
参考文献
Lednicer; Von Voigtlander; Emmert
Journal of Medicinal Chemistry, 1981 , vol. 24, # 4 p. 404 - 408
