1-溴-2-甲基-3,5-二硝基苯合成路线 (共 4 条)
反应条件
N-bromosuccinmide; sulfuric acid T=80°C; 0.75 h;
参考文献
Kim, Mi Kyoung; Shin, Heerim; Cho, Seo Young; Chong, Youhoon
Bioorganic and Medicinal Chemistry, 2014 , vol. 22, # 3 p. 1156 - 1162
反应条件
sulfuric acid; bromine; nitric acid T=90°C; 0.166667 h; Title compound not separated from byproducts;
参考文献
Melhuish, Martin W.; Moodie, Roy B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 667 - 674
反应条件
sulfuric acid; nitric acid; chlorine T=90°C; 0.8 h; further reaction times; oleum instead of sulphuric acid; Rate constantMechanismProduct distribution;
参考文献
Melhuish, Martin W.; Moodie, Roy B.
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1989 , p. 667 - 674
反应条件
sodium dichromate; sulfuric acid
参考文献
Segura, Pascual; Bunnett, Joseph F.; Villanova, Laura
Journal of Organic Chemistry, 1985 , vol. 50, # 7 p. 1041 - 1045