(4-氯苯基)(二甲基)硅烷醇合成路线 （共 8 条）
反应条件
hydrogenchloride in 1,4-dioxane T=25°C; 1 h; var. of reagent; Rate constantEquilibrium constant;
参考文献
Kohlheim; Lange; Kelling
Advanced Synthesis and Catalysis, 1996 , vol. 338, # 7 p. 660 - 662
反应条件
water; silver(I) acetate in acetonitrile
T=50°C; P=760.051 Torr; 1 h;
参考文献
Kikukawa, Yuji; Kuroda, Yoshiyuki; Yamaguchi, Kazuya; Mizuno, Noritaka
Angewandte Chemie - International Edition, 2012 , vol. 51, # 10 p. 2434 - 2437
反应条件
1: 1-chloro-4-bromobenzene With tert.-butyl lithium in diethyl ether
T=-78 - -60°C; Inert atmosphere;
2: cyclo-(Me2SiO)3 in diethyl ether
T=-74°C; Inert atmosphere;
参考文献
Denmark, Scott E.; Smith, Russell C.; Chang, Wen-Tau T.; Muhuhi, Joseck M.
Journal of the American Chemical Society, 2009 , vol. 131, # 8 p. 3104 - 3118
反应条件
1: With 2,2,6,6-tetramethyl-piperidine-N-oxyl; potassium bromide in acetone
T=20°C; 0.166667 h;
2: With sodium hypochlorite; sodium hydrogencarbonate in water; acetone
T=20°C; 1 h;
参考文献
Takeda, Daisuke; Oyama, Ryo; Yamada, Shozo
Chemistry Letters, 2009 , vol. 38, # 6 p. 532 - 533
参考文献
Mitsudome, Takato; Noujima, Akifumi; Mizugaki, Tomoo; Jitsukawa, Koichiro; Kaneda, Kiyotomi
Chemical Communications, 2009 , # 35 p. 5302 - 5304
反应条件
hydrogenchloride in 1,4-dioxane
T=25°C; 1 h; Equilibrium constant;
参考文献
Kohlheim; Lange; Kelling
Advanced Synthesis and Catalysis, 1996 , vol. 338, # 7 p. 660 - 662
参考文献
Aoki, Toshiki; Watanabe, Jun; Ishimoto, Yoshiyuki; Oikawa, Eizo; Hayakawa, Yoshio; Nishida, Masakazu
Journal of Fluorine Chemistry, 1992 , vol. 59, # 2 p. 285 - 288
反应条件
1: 1.) Mg
2: NH4OH
View Scheme
参考文献
Aoki, Toshiki; Watanabe, Jun; Ishimoto, Yoshiyuki; Oikawa, Eizo; Hayakawa, Yoshio; Nishida, Masakazu
Journal of Fluorine Chemistry, 1992 , vol. 59, # 2 p. 285 - 288
