5-三甲基甲硅烷基-2-噻吩羧酸合成路线 （共 9 条）
参考文献
Benkeser; Currie
Journal of the American Chemical Society, 1948 , vol. 70, p. 1780
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Gmelin Handbook: Si: MVol.C, 30, page 94 - 96
反应条件
n-butyllithium; diethyl ether anschliessend Behandeln mit festem Kohlendioxid;
参考文献
Gmelin Handbook: Si: MVol.C, 30, page 94 - 96
参考文献
Knight, David W.; Nott, Andrew P.
Tetrahedron Letters, 1980 , vol. 21, p. 5051 - 5054
反应条件
diethyl ether; magnesium anschliessend Behandeln mit festem Kohlendioxid;
参考文献
Benkeser; Torkelson
Journal of the American Chemical Society, 1954 , vol. 76, p. 1252
反应条件
sodium hydroxide; iodine
参考文献
Benkeser; Currie
Journal of the American Chemical Society, 1948 , vol. 70, p. 1780
反应条件
1: Lithium diisopropylamide / tetrahydrofuran / -78 °C 2: 85 percent / -78 °C View Scheme
参考文献
Knight, David W.; Nott, Andrew P.
Tetrahedron Letters, 1980 , vol. 21, p. 5051 - 5054
反应条件
lithium diisopropyl amide 1.) THF, -78 deg C, 10 min, 2.) 0.5 h; Yield given. Multistep reaction;
参考文献
Knight, David W.; Nott, Andrew P.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1983 , p. 791 - 794
参考文献
Benkeser; Currie
Journal of the American Chemical Society, 1948 , vol. 70, p. 1780
反应条件
HCl in neat (no solvent)
byproducts: 2-thiophene-carboxylic acid; (CH3)3Si(C4H2S(COOH)) and gaseous HCl;;
参考文献
Benkeser; Currie
Journal of the American Chemical Society, 1948 , vol. 70, p. 1780
Full Text View citing articles Show Details
Gmelin Handbook: Si: MVol.C, 30, page 94 - 96
