4-叔丁基硫杂杯[4]芳烃合成路线 （共 18 条）
反应条件
potassium phosphate; copper(l) iodide in toluene T=80°C; 5 h;
参考文献
Journal of Organic Chemistry, , vol. 76, # 7 p. 2168 - 2179
反应条件
potassium phosphate; copper(l) iodide; ethylene glycol in toluene T=80°C; 3 h;
参考文献
Journal of Organic Chemistry, , vol. 76, # 7 p. 2168 - 2179
反应条件
1: With 1-Hexylamine in benzene Heating; 2: With sodium carbonate in N,N-dimethyl-formamide Heating;
参考文献
Russian Chemical Bulletin, , vol. 60, # 3 p. 486 - 498
反应条件
sodium perborate in chloroform; acetic acid T=50°C; 18 h;
参考文献
Morohashi, Naoya; Iki, Nobuhiko; Sugawara, Atsushi; Miyano, Sotaro
Tetrahedron, 2001 , vol. 57, # 26 p. 5557 - 5563
反应条件
1: With sodium tungstate hydrate; dihydrogen peroxide; sodium acetate; acetic acid in water T=60 - 80°C; 23.5 h; 2: With hydrogenchloride in water T=80°C; Product distribution / selectivity;
参考文献
HODOGAYA CHEMICAL CO., LTD.
Patent: US2009/275783 A1, 2009 ;
Location in patent: Page/Page column 4-5 ;
反应条件
caesium carbonate in acetone Substitution; 4 h; Heating;
参考文献
Iki, Nobuhiko; Narumi, Fumitaka; Fujimoto, Toyohisa; Morohashi, Naoya; Miyano, Sotaro
Journal of the Chemical Society. Perkin Transactions 2, 1998 , # 12 p. 2745 - 2750
反应条件
1: p-tert-butylthiacalix[4]arene With potassium carbonate; potassium iodide in acetone 0.5 h; RefluxInert atmosphere; 2: chloroacetic acid ethyl ester in acetone 120 h; Reflux;
参考文献
Liu, Li; Huang, Kun; Yan, Chao Guo
Journal of Inclusion Phenomena and Macrocyclic Chemistry, 2010 , vol. 66, # 3 p. 349 - 355
反应条件
sodium carbonate in acetone 24 h; Heating;
参考文献
Van Leeuwen, Fijs W. B.; Beijleveld, Hans; Velders, Aldrik H.; Huskens, Jurriaan; Verboom, Willem; Reinhoudt, David N.
Organic and Biomolecular Chemistry, 2005 , vol. 3, # 10 p. 1993 - 2001
