in dichloromethane WCl6 suspd. in CH2Cl2, soln. of Si compd. in CH2Cl2 added over a 4-h period under N2; filtration, washing with pentane, drying in vac., removal of CH2Cl2 from filtrate in vac., sublimation at 80°C;
参考文献
Pederson,S.F.; Schrock,R.R.
Journal of the American Chemical Society, 1982 , vol. 104, p. 7483
Hayes, Roger N.; Bowie, John H.; Klass, Gunter
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 7 p. 1167 - 1174
products detemination by I.c.r. method, var. esters;;
参考文献
Hayes, Roger N.; Bowie, John H.; Klass, Gunter
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 7 p. 1167 - 1174
Hayes, Roger N.; Bowie, John H.; Klass, Gunter
Journal of the Chemical Society, Perkin Transactions 2: Physical Organic Chemistry (1972-1999), 1984 , # 7 p. 1167 - 1174
hexamethyldistannoxane in pyridine-D5
P=0.001 Torr; 12 h;
参考文献
Zemlyansky, N. N.; Borisova, I. V.; Shestakova, A. K.; Ustynyuk, Yu. A.; Chernyshev, E. A.
Russian Chemical Bulletin, 1994 , vol. 43, p. 2126 - 2127
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1994 , # 12 p. 2246 - 2247
hexamethyldistannoxane in pyridine-D5
T=20°C; P=0.001 Torr; 12 h;
参考文献
Zemlyansky, N. N.; Borisova, I. V.; Shestakova, A. K.; Ustynyuk, Yu. A.; Chernyshev, E. A.
Russian Chemical Bulletin, 1994 , vol. 43, p. 2126 - 2127
Izvestiya Akademi Nauk, Seriya Khimicheskaya, 1994 , # 12 p. 2246 - 2247
