反应条件
in dichloromethane
byproducts: trimethylchlorosilane; reaction with three or more equiv. trimethylmethoxysilane at -78°C. The mixture was allowed to warm to room temp., concg. under reduced pressure, then hexane was added to give a white cryst. solid (all operations in an inert atmosphere); washing with hexane, dried under vac., elem.anal.;
参考文献
Antinolo, A.; Otero, A.; Urbanos, F.; Garcia-Blanco, S.; Martinez-Carrera, S.; Sanz-Aparicio, J.
Journal of Organometallic Chemistry, 1988 , vol. 350, p. 25 - 34
