methanol in diethyl ether To stibane compound in Et2O is added under Ar methanol at -50°C, the soln. is stirred for 0.5 h.; removal of volatiles under vac.;
参考文献
Ates, M.; Breunig, H. J.; Guelec, S.
Phosphorus, Sulfur and Silicon and the Related Elements, 1989 , vol. 44, p. 129 - 134
methanol in benzene To methanol is added stibane compound in benzene under Ar and the soln. is stirred at 25°C for 2 h.; removal of volatiles under vac.;
参考文献
Ates, M.; Breunig, H. J.; Guelec, S.
Phosphorus, Sulfur and Silicon and the Related Elements, 1989 , vol. 44, p. 129 - 134
