反应条件
in neat (no solvent)
Schlenk techniques used; dry oxygen-free nitrogen or argon atm.; supension of (Nb(η5-C5H4Si(CH3)3)2Cl2)PF6 in Me3SiOCH2CH3; stirring (3 h/room temp.); initial red solid turns yellow;; filtration; washing (hexane); recrystn. (dissolving in chloroform/overlayered by hexane/few days); elem anal.;;
参考文献
Antinolo, Antonio; Fajardo, Mariano; Otero, Antonio; Mugnier, Yves; Nabaoui, Hassane; Mourad, Houssef
Journal of Organometallic Chemistry, 1991 , vol. 414, # 2 p. 155 - 164
