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乙二醇
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63148-62-9
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二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-苯基噻唑
合成路线
（共 33 条）
57516-16-2
2-溴-4-苯基噻唑
→
反应条件
1826-12-6
4-苯基噻唑
反应条件
sodium tetrahydroborate; N,N,N',N,-tetramethylethylenediamine; palladium diacetate; triphenylphosphine in tetrahydrofuran T=20°C; 3 h; Inert atmosphere; Reagent/catalystTime;
参考文献
Chelucci, Giorgio; Baldino, Salvatore; Ruiu, Andrea
Journal of Organic Chemistry, 2012 , vol. 77, # 21 p. 9921 - 9925,5
1403935-14-7
→
反应条件
1826-12-6
4-苯基噻唑
反应条件
sodium tetrahydroborate; N,N,N',N,-tetramethylethylenediamine; PdCl2(1,1′-bis(di-tertbutylphosphino)ferrocene) in tetrahydrofuran T=65°C; 20 h; Inert atmosphere; Reagent/catalystTimeTemperature;
参考文献
Chelucci, Giorgio; Baldino, Salvatore; Ruiu, Andrea
Journal of Organic Chemistry, 2012 , vol. 77, # 21 p. 9921 - 9925,5
1826-23-9
2-氯-4-苯基噻唑
→
反应条件
1826-12-6
4-苯基噻唑
反应条件
sodium tetrahydroborate; dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct; N,N,N',N,-tetramethylethylenediamine in tetrahydrofuran T=20°C; 22 h; Inert atmosphere; Reagent/catalystTime;
参考文献
Chelucci, Giorgio; Baldino, Salvatore; Ruiu, Andrea
Journal of Organic Chemistry, 2012 , vol. 77, # 21 p. 9921 - 9925,5
188585-15-1
→
反应条件
59278-68-1
+
1826-12-6
4-苯基噻唑
反应条件
sodium tetrahydroborate; N,N,N',N,-tetramethylethylenediamine; palladium diacetate; triphenylphosphine in tetrahydrofuran T=0°C; 14 h; Inert atmosphere; Reagent/catalystTime; regioselective reaction;
参考文献
Journal of Organic Chemistry, , vol. 77, # 21 p. 9921 - 9925,5
57516-16-2
2-溴-4-苯基噻唑
→
反应条件
1826-12-6
4-苯基噻唑
+
4072-63-3
+
111600-96-5
反应条件
triethylamine; ethyl acrylate; palladium diacetate in N,N-dimethyl-formamide T=130°C; 24 h; sealed tube;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 35, # 2 p. 823 - 828
57516-16-2
2-溴-4-苯基噻唑
→
反应条件
1826-12-6
4-苯基噻唑
+
4072-63-3
+
111600-97-6
反应条件
triethylamine; acrylonitrile; palladium diacetate in N,N-dimethyl-formamide T=100°C; 48 h; sealed tube;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 35, # 2 p. 823 - 828
140-88-5
丙烯酸乙酯
+
57516-16-2
2-溴-4-苯基噻唑
→
反应条件
1826-12-6
4-苯基噻唑
+
4072-63-3
+
111600-96-5
反应条件
triethylamine; palladium diacetate in N,N-dimethyl-formamide T=130°C; 24 h; sealed tube;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 35, # 2 p. 823 - 828
292638-84-7
+
57516-16-2
2-溴-4-苯基噻唑
→
反应条件
1826-12-6
4-苯基噻唑
+
111600-99-8
反应条件
triethylamine; palladium diacetate in N,N-dimethyl-formamide T=100°C; 48 h; sealed tube;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 35, # 2 p. 823 - 828
107-13-1
丙烯腈
+
57516-16-2
2-溴-4-苯基噻唑
→
反应条件
1826-12-6
4-苯基噻唑
+
4072-63-3
+
111600-97-6
反应条件
triethylamine; palladium diacetate in N,N-dimethyl-formamide T=100°C; 48 h; sealed tube;
参考文献
Chemical and Pharmaceutical Bulletin, , vol. 35, # 2 p. 823 - 828
2010-06-2
2-氨基-4-苯基噻唑
→
反应条件
1826-12-6
4-苯基噻唑
反应条件
tetrahydrofuran; oxygen; nitrogen(II) oxide 8 h; Ambient temperature;
参考文献
Itoh, Takashi; Matsuya, Yuji; Nagata, Kazuhiro; Ohsawa, Akio
Chemical and Pharmaceutical Bulletin, 1997 , vol. 45, # 9 p. 1547 - 1549
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