4-(4-硝基苯基)哌嗪-1-羧酸叔丁酯合成路线 (共 14 条)
反应条件
hydrogen; palladium 10 on activated carbon in methanol; ethyl acetate P=760.051 Torr; 2 h;
参考文献
WO2006/38039 A1, ;
Page/Page column 17; 30 ;
反应条件
palladium in ethanol
参考文献
US5556969 A1, ;
US 5556969 A
反应条件
hydrogen in tetrahydrofuran
参考文献
US2003/73668 A1, ;
US 20030073668 A1
反应条件
1: trifluoroacetic acid / dichloromethane / 1 h / 20 °C
2: triethylamine / dichloromethane / 1 h / 0 - 5 °C
View Scheme
参考文献
AURIGENE DISCOVERY TECHNOLOGIES LIMITED; SENGUPTA, Saumitra; RAJAGOPALAN, Srinivasan; BELAVAGI, Ningaraddi; RAMACHANDRA, Muralidhara
Patent: WO2012/59932 A1, 2012 ;
WO 2012/059932 A1