顺-1,2-(2-噻嗯基)二乙烯合成路线 （共 5 条）
反应条件
titanium tetrachloride; zinc in tetrahydrofuran T=0°C; 4.25 h;
参考文献
Gwangju Institute of Science and Technology
Patent: EP2065389 A1, 2009 ;
Location in patent: Page/Page column 5-6 ;
反应条件
sodium hydride in ethylene glycol dimethyl ether; mineral oil T=0 - 20°C; Horner-Wadsworth-Emmons olefination; Inert atmosphereDarkness;
参考文献
Younes, Ali H.; Zhang, Lu; Clark, Ronald J.; Davidson, Michael W.; Zhu, Lei
Organic and Biomolecular Chemistry, 2010 , vol. 8, # 23 p. 5431 - 5441
反应条件
Ag2CrO4; sodium hydride in diethylene glycol dimethyl ether T=130°C; 0.166667 h;
参考文献
Heterocycles, , vol. 26, # 7 p. 1891 - 1898
反应条件
dirhodium tetraacetate in tetrahydrofuran T=-20 - 0°C; 0.166667 h; cis/trans ratio 2.7; Yield given;
参考文献
Tetrahedron Letters, , vol. 23, # 22 p. 2277 - 2280
反应条件
Mo(N-2,6-iPr2C6H3)(CHCMe2Ph)(OCMe(CF3)2)2 in toluene 1:1 ratio of reagents, vinylferrocene/catalyst: 60-100 at room temp. for15 h under Ar atmosphere, self- and cross-metathesis;
参考文献
Yasuda, Tomohiro; Abe, Jiro; Iyoda, Tomokazu; Kawai, Tadashi
Chemistry Letters, 2001 , # 8 p. 812 - 813
