2,2,3,4,4,5-六溴联苯醚合成路线 （共 8 条）
反应条件
sodium hydroxide in water 2 h; Heating;
参考文献
Liu, Huiling; Bernhardsen, Monica; Fiksdahl, Anne
Tetrahedron, 2006 , vol. 62, # 15 p. 3564 - 3572
反应条件
1.1: 64.9 percent / bromine; Fe / CH2Cl2 / Heating 2.1: sulfuric acid; acetic acid; acetic acid anhydride / CrO3 / 0 - 25 °C 3.1: 0 - 20 °C 3.2: methanol; H2O / 1 h 3.3: NaBr / H2O / 3 h 4.1: 54 percent / sodium hydroxide / H2O / 2 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 62, # 15 p. 3564 - 3572
反应条件
1.1: sulfuric acid; acetic acid; acetic acid anhydride / CrO3 / 0 - 25 °C 2.1: 0 - 20 °C 2.2: methanol; H2O / 1 h 2.3: NaBr / H2O / 3 h 3.1: 54 percent / sodium hydroxide / H2O / 2 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 62, # 15 p. 3564 - 3572
反应条件
bromine; iron in tetrachloromethane Heating;
参考文献
Acta Chemica Scandinavica, , vol. 50, p. 802 - 807
反应条件
1: bromine; acetic acid / 1.5 h / 20 °C 2: bromine; acetic acid / 1.5 h / 20 °C 3: 54 percent / sodium hydroxide / H2O / 2 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 62, # 15 p. 3564 - 3572
反应条件
1: bromine; acetic acid / 1.5 h / 20 °C 2: 54 percent / sodium hydroxide / H2O / 2 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 62, # 15 p. 3564 - 3572
反应条件
1: 81.7 percent / potassium hydroxide / methanol / 24 h / Heating 2: 54 percent / sodium hydroxide / H2O / 2 h / Heating View Scheme
参考文献
Tetrahedron, , vol. 62, # 15 p. 3564 - 3572
反应条件
1: 1.) potassium hydroxide, 2.) copper bronze / 1.) 10 min, 2.) 170 deg C, 2 h 2: 45 percent / bromine, iron / CCl4 / Heating View Scheme
参考文献
Acta Chemica Scandinavica, , vol. 50, p. 802 - 807
