2-氯-4-羟基-5-甲氧基苯甲醛合成路线 （共 15 条）
反应条件
sodium hydroxide; dihydrogen peroxide
参考文献
Oliverio; Castelfranchi
Gazzetta Chimica Italiana, 1950 , vol. 80, p. 267
Full Text Show Details
Asp; Lindberg
Acta Chemica Scandinavica (1947-1973), 1950 , vol. 4, p. 60,61
参考文献
Jayne
Journal of the American Chemical Society, 1953 , vol. 75, p. 1742
反应条件
1: 1.1 g / pyridine / 18 h / 20 °C
2: 460 mg / diethyl ether / 48 h / 20 °C
3: 120 mg / sodium methoxide / methanol / 1 h / Heating
View Scheme
参考文献
Jayne
Journal of the American Chemical Society, 1953 , vol. 75, p. 1742
反应条件
potassium carbonate in N,N-dimethyl-formamide
T=60°C; 18 h;
参考文献
Carvalho, Christopher F.; Sargent, Melvyn V.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1984 , # 8 p. 1913 - 1918
反应条件
boron tribromide in dichloromethane
T=20°C; demethylation; 4 h;
参考文献
Hyotylainen
Chemosphere, 1994 , vol. 28, # 9 p. 1641 - 1656
