反应条件
in hexane
byproducts: LiCl; under Ar, dropwise addn. of Li-compd. in hexane within 2 h to a hexane soln. of borane, stirred for 16 h at room temp.; centrifuged, distn. of volatiles in vac., taken up in hexane, cooled to -78°C for 48 h, isolation at -78°C, washed with hexane (-78°C); elem. anal.;
参考文献
Kroner, Juergen; Noeth, Heinrich; Polborn, Kurt; Stolpmann, Holger; Tacke, Matthias; Thomann, Martina
Chemische Berichte, 1993 , vol. 126, p. 1995 - 2002
