4-羟基-2-甲氧基苯甲醛合成路线 (共 36 条)
反应条件
potassium fluoride; thiophenol in 1-methyl-pyrrolidin-2-one T=100°C; 1 h;
参考文献
Chakraborti, Asit K.; Sharma, Lalima; Nayak, Mrinal K.
Journal of Organic Chemistry, 2002 , vol. 67, # 8 p. 2541 - 2547
反应条件
potassium hydroxide in chloroform 3 h; Heating;
参考文献
Patel; Richardson
Carbohydrate research, 1986 , vol. 146, # 2 p. 241 - 249
反应条件
potassium fluoride; thiophenol in 1-methyl-pyrrolidin-2-one T=100°C; 1 h;
参考文献
Chakraborti, Asit K.; Sharma, Lalima; Nayak, Mrinal K.
Journal of Organic Chemistry, 2002 , vol. 67, # 8 p. 2541 - 2547
反应条件
4-MeC6H4SNa in dimethyl sulfoxide T=20°C; 2.08333 h;
参考文献
Chapman, Erin E.; Langler, Richard F.
Journal of Sulfur Chemistry, 2010 , vol. 31, # 1 p. 19 - 26
反应条件
in ethanol; water T=210°C; P=30003 Torr; 1.5 h; Microwave irradiationAutoclave;
参考文献
Jeon, Jae-Ho; Kim, Mi Ran; Jun, Jong-Gab
Synthesis, 2011 , # 3 art. no. F18510SS, p. 370 - 376
反应条件
trichlorophosphate T=0 - 5°C; Further byproducts given;
参考文献
Mergler, M.; Tanner, R.; Gosteli, J.; Grogg, P.
Tetrahedron Letters, 1988 , vol. 29, # 32 p. 4005 - 4008
反应条件
trifluorormethanesulfonic acid in 1,2-dichloro-ethane T=-40 - 40°C; Fries rearrangement; 12.5 h; Title compound not separated from byproducts;
参考文献
Zeitschrift fur Naturforschung - Section B Journal of Chemical Sciences, , vol. 56, # 11 p. 1178 - 1187
反应条件
1: alkali 2: hydrogen chloride; aluminium chloride View Scheme
参考文献
Chemische Berichte, , vol. 55, p. 928
反应条件
hydrogenchloride; aluminium trichloride; benzene T=35 - 40°C; Behandeln des Reaktionsprodukts mit salzsaeurehaltigem Wasser beim Erhitzen;
参考文献
Justus Liebigs Annalen der Chemie, , vol. 357, p. 373
Chemische Berichte, , vol. 31, p. 1767
DE101333 ;
反应条件
trichlorophosphate T=-12 - 15°C; Vilsmeier formylation;
参考文献
Novikova; Kilimenchuk; Kondrat'Eva; Meshkova; Topilova
Russian Journal of Applied Chemistry, 2011 , vol. 84, # 6 p. 978 - 983