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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
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乙二醇
甲醛
63148-62-9
MDI
丁酮
二甲基亚砜
碳酸氢钠
471-34-1
4-碘苄醇
合成路线
（共 87 条）
288-32-4
咪唑
+
18282-51-4
4-碘苄醇
→
反应条件
86718-08-3
4-(1-咪唑基)苄醇
反应条件
potassium phosphate; copper(l) iodide in N,N-dimethyl-formamide T=35 - 40°C; 40 h; Inert atmosphere; chemoselective reaction;
参考文献
Zhu, Liangbo; Li, Gaocan; Luo, Liang; Guo, Peng; Lan, Jingbo; You, Jingsong
Journal of Organic Chemistry, 2009 , vol. 74, # 5 p. 2200 - 2202
18282-51-4
4-碘苄醇
→
反应条件
87736-88-7
4-[3-(三氟甲基)-3H-双吖丙啶-3-基]苄醇
反应条件
1.1: 1H-imidazole / N,N-dimethyl-formamide / 2 h / 20 °C 2.1: n-butyllithium / tetrahydrofuran; hexane / 0.75 h / -78 °C 2.2: 1.25 h / -78 °C 3.1: pyridine; hydroxylamine hydrochloride / ethanol / 60 °C 4.1: triethylamine; 4-(N,N-dimethlyamino)pyridine / dichloromethane / 20 °C 5.1: ammonium hydroxide / tetrahydrofuran / 48 h / -78 - 20 °C / |Sealed tube 6.1: triethylamine; iodine / methanol / 20 °C 7.1: tetrabutyl ammonium fluoride / tetrahydrofuran / 1 h / 20 °C View Scheme
参考文献
Journal of Organic Chemistry, , vol. 79, # 6 p. 2463 - 2472
18282-51-4
4-碘苄醇
→
反应条件
78712-43-3
盐酸奥扎格雷
反应条件
1: tetra-n-butylammonium acetate; triethylamine / 48 h / 140 °C / |Inert atmosphere 2: 1-methyl-pyrrolidin-2-one / 1 h / 170 °C 3: sodium hydroxide / water; methanol / 2 h / 25 °C View Scheme
参考文献
Yamada, Yoichi M. A.; Yuyama, Yoshinari; Sato, Takuma; Fujikawa, Shigenori; Uozumi, Yasuhiro
Angewandte Chemie - International Edition, 2014 , vol. 53, # 1 p. 127 - 131
Angew. Chem., 2014 , vol. 126, # 01 p. 5131 - 5135
18282-51-4
4-碘苄醇
→
反应条件
59528-27-7
4-碘苄胺盐酸盐
反应条件
1: 84 percent / DEAD; PPh3 / tetrahydrofuran; toluene / 20 °C 2: 100 percent / NH2NH2*H2O; aq. HCl / methanol / Heating View Scheme
参考文献
Lee, Shoukou; Shinji, Chihiro; Ogura, Kiyoshi; Shimizu, Motomu; Maeda, Satoko; Sato, Mayumi; Yoshida, Minoru; Hashimoto, Yuichi; Miyachi, Hiroyuki
Bioorganic and Medicinal Chemistry Letters, 2007 , vol. 17, # 17 p. 4895 - 4900
18282-51-4
4-碘苄醇
+
108-98-5
硫酚
→
反应条件
6317-56-2
对苯硫基苯甲醇
反应条件
CyPF-tBu; palladium diacetate; caesium carbonate in ethylene glycol dimethyl ether T=110°C; Inert atmosphere;
参考文献
Fernandez-Rodriguez, Manuel A.; Hartwig, John F.
Journal of Organic Chemistry, 2009 , vol. 74, # 4 p. 1664 - 1672
18282-51-4
4-碘苄醇
→
反应条件
623-04-1
对氨基苯甲醇
反应条件
ammonium hydroxide; potassium phosphate; 1-(5,6,7,8-tetrahydroquinolin-8-yl)-2-methylpropan-1-one; copper(I) bromide in dimethyl sulfoxide T=25°C; 24 h; Inert atmosphereSealed tube;
参考文献
Wang, Deping; Cai, Qian; Ding, Ke
Advanced Synthesis and Catalysis, 2009 , vol. 351, # 11-12 p. 1722 - 1726
18282-51-4
4-碘苄醇
→
反应条件
53339-53-0
4-巯基苯甲醇
反应条件
1: With copper(l) iodide; potassium carbonate; sulfur in N,N-dimethyl-formamide T=90°C; 12 h; Inert atmosphere; 2: With sodium tetrahydroborate in N,N-dimethyl-formamide T=40°C; Inert atmosphereCooling with ice;
参考文献
Jiang, Yongwen; Qin, Yuxia; Xie, Siwei; Zhang, Xiaojing; Dong, Jinhua; Ma, Dawei
Organic Letters, 2009 , vol. 11, # 22 p. 5250 - 5253
18282-51-4
4-碘苄醇
→
反应条件
624-31-7
4-碘甲苯
反应条件
cis-IrCl(CO)(PPh3)2; hydrazine hydrate; potassium hydroxide in methanol T=160°C; Wolff-Kishner Reduction; 3 h; Sealed tube;
参考文献
Huang, Jian-Lin; Dai, Xi-Jie; Li, Chao-Jun
European Journal of Organic Chemistry, 2013 , # 29 p. 6496 - 6500
18282-51-4
4-碘苄醇
+
106-95-6
3-溴丙烯
→
反应条件
14593-43-2
烯丙基苄基醚
+
100-51-6
苯甲醇
反应条件
1: 4-iodobenzenemethanol With tert.-butyl lithium in tetrahydrofuran T=0°C; 0.5 h; 2: allyl bromide in tetrahydrofuran T=20°C; 12 h;
参考文献
Uchiyama, Masanobu; Furuyama, Taniyuki; Kobayashi, Minoru; Matsumoto, Yotaro; Tanaka, Kentaro
Journal of the American Chemical Society, 2006 , vol. 128, # 26 p. 8404 - 8405
18282-51-4
4-碘苄醇
→
反应条件
138500-85-3
4-溴甲基苯硼酸频哪醇酯
反应条件
1: potassium acetate / dichloro(1,1'-bis(diphenylphosphanyl)ferrocene)palladium(II) dichloromethane adduct / dimethyl sulfoxide / 18 h / 85 °C / Inert atmosphere 2: triethylamine / dichloromethane / 2 h / 0 °C / Inert atmosphere 3: potassium bromide / N,N-dimethyl-formamide / 19 h / 20 °C / Inert atmosphere View Scheme
参考文献
Riken
Patent: EP2450354 A1, 2012 ;
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