双三甲基硅基化乙烯基磷酸酯合成路线 （共 10 条）
反应条件
in dichloromethane T=20°C; 3.33333 h;
参考文献
Wyeth
Patent: US2006/79679 A1, 2006 ;
Location in patent: Page/Page column 15 ;
参考文献
Gutierrez; Prisbe; Rohloff
Nucleosides, Nucleotides and Nucleic Acids, 2001 , vol. 20, # 4-7 p. 1299 - 1302
反应条件
in tetrachloromethane T=0 - 10°C;
参考文献
Blackburn, G. Michael; Ingleson, David
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1980 , p. 1150 - 1153
反应条件
trimethylsilyl bromide
参考文献
McKenna,C.E. et al.
Tetrahedron Letters, 1977 , # 2 p. 155 - 158
反应条件
in dichloromethane Inert atmosphere;
参考文献
Czakler, Matthias; Artner, Christine; Schubert, Ulrich
European Journal of Inorganic Chemistry, 2014 , # 12 p. 2038 - 2045
参考文献
Gross,H. et al.
Journal fuer Praktische Chemie (Leipzig), 1978 , vol. 320, p. 344 - 350
反应条件
phosphorus pentachloride in dichloromethane 1 h;
参考文献
Wyeth
Patent: US2006/79679 A1, 2006 ;
Location in patent: Page/Page column 15 ;
反应条件
phosphorus pentachloride in tetrachloromethane 0.5 h; Ambient temperature;
参考文献
Morita, Tsuyoshi; Okamoto, Yoshiki; Sakurai, Hiroshi
Chemistry Letters, 1980 , p. 435 - 438
参考文献
Gutierrez; Prisbe; Rohloff
Nucleosides, Nucleotides and Nucleic Acids, 2001 , vol. 20, # 4-7 p. 1299 - 1302
反应条件
phosphorus pentachloride in tetrachloromethane
0.5 h; Ambient temperature;
参考文献
Morita, Tsuyoshi; Okamoto, Yoshiki; Sakurai, Hiroshi
Chemistry Letters, 1980 , p. 435 - 438
