三甲基(3-甲基-2-丁烯-1-基)-硅烷合成路线 （共 58 条）
反应条件
zinc(II) chloride in dichloromethane
T=25°C; 42 h;
参考文献
Yokozawa; Furuhashi; Natsume
Tetrahedron Letters, 1995 , vol. 36, # 29 p. 5243 - 5246
反应条件
Ph3C+ClO4- in dichloromethane
T=-45°C; 3 h; Yield given. Yields of byproduct given;
参考文献
Murakami, Masahiro; Kato, Takashi; Mukaiyama, Teruaki
Chemistry Letters, 1987 , p. 1167 - 1170
反应条件
trimethylsilyl trifluoromethanesulfonate in chloroform
T=40°C; Sakurai-Hosomi reaction; 9 h;
参考文献
Kobashi, Yohei; Minowa, Tomofumi; Mukaiyama, Teruaki
Chemistry Letters, 2005 , vol. 34, # 6 p. 756 - 757
反应条件
in acetonitrile
T=25°C; 0.166667 h; Irradiation; Quantum yieldProduct distribution;
参考文献
Ohga, Kazuya; Yoon, Ung Chan; Mariano, Patrick S.
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 213 - 219
反应条件
trimethylsilylazide; iodosylbenzene; boron trifluoride diethyl etherate in dichloromethane
T=-78°C; 0.5 h; Yield given. Yields of byproduct given;
参考文献
Arimoto, Masao; Yamaguchi, Hideo; Fujita, Eiichi; Ochiai, Masahito; Nagao, Yoshimitsu
Tetrahedron Letters, 1987 , vol. 28, # 50 p. 6289 - 6292
反应条件
1.1: AlCl3 / CH2Cl2 / 0.5 h / 0 °C
1.2: 78 percent / CH2Cl2 / 0.17 h / -60 °C
2.1: 50 percent / p-TsOH / [Rh(cod)Cl]2 / CH2Cl2 / 20 h / 100 °C / 60004.8 Torr
View Scheme
参考文献
Keraenen, Mark D.; Kot, Kinga; Hollmann, Christoph; Eilbracht, Peter
Organic and Biomolecular Chemistry, 2004 , vol. 2, # 22 p. 3379 - 3384
反应条件
in acetonitrile
Irradiation;
参考文献
Ohga, Kazuya; Mariano, Patrick S.
Journal of the American Chemical Society, 1982 , vol. 104, # 2 p. 617 - 619
反应条件
in acetonitrile
T=25°C; 0.166667 h; Irradiation; Quantum yieldProduct distribution;
参考文献
Ohga, Kazuya; Yoon, Ung Chan; Mariano, Patrick S.
Journal of Organic Chemistry, 1984 , vol. 49, # 2 p. 213 - 219
反应条件
oxygen O2, singlet in methanol
T=40°C; 0.5 h; Irradiation; Title compound not separated from byproducts;
参考文献
Dubac, J.; Laporterie, A.; Iloughmane, H.; Pillot, J. P.; Deleris, G.; Dunogues, J.
Journal of Organometallic Chemistry, 1985 , vol. 281, p. 149 - 162
反应条件
boron trifluoride diethyl etherate; triphenylbismuth(V) difluoride in dichloromethane
-78 deg C -> r.t.;
参考文献
Matano, Yoshihiro; Yoshimune, Masanori; Suzuki, Hitomi
Tetrahedron Letters, 1995 , vol. 36, # 41 p. 7475 - 7478
