anhydrous magnesium perchlorate; NADH model 2 in acetonitrile T=60°C; var. equivalent amount of Mg2+; Product distribution;

anhydrous magnesium perchlorate; NADH model 2 in acetonitrile T=60°C;

<b>Multi-step reaction with 2 steps<br /> </b>1: 1.) nBuLi, 3.) 10percent aq. ammonium chloride, 4.) sulfuric acid, gl. acetic acid<br />2: 30 percent / sodium nitrite, iodine / ethane-1,2-diol; H₂O; ethyl acetate / 72 h / 20 &deg;C<br /> <br /> &nbsp;

<b>With</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3587194', constants.ctx, '0')">iodine</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '906771', constants.ctx, '0')">sodium nitrite</a>&nbsp;<b>in</b>&nbsp; <a href="#" onclick="return RXDsubstances(event, this, '3587155', constants.ctx, '0')">water</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '505945', constants.ctx, '0')">ethylene glycol</a>;&nbsp;<a href="#" onclick="return RXDsubstances(event, this, '506104', constants.ctx, '0')">ethyl acetate</a> <br />T=20&deg;C;&nbsp;72&nbsp;h;&nbsp;<br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: 1.) nBuLi, 3.) 10percent aq. ammonium chloride, 4.) sulfuric acid, gl. acetic acid<br />2: 30 percent / sodium nitrite, iodine / ethane-1,2-diol; H₂O; ethyl acetate / 72 h / 20 &deg;C<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: diethyl ether / 2 h / Heating<br />2: 4 h / Heating<br /> <br /> &nbsp;

<b>Multi-step reaction with 2 steps<br /> </b>1: diethyl ether / 2 h / Heating<br />2: 4 h / Heating<br /> <br /> &nbsp;