甲基3-(三甲基硅烷基)丙酸酯合成路线 （共 7 条）
反应条件
dicobalt octacarbonyl in benzene T=25°C; 3 h;
参考文献
Takeshita, Kenji; Seki, Yoshio; Kawamoto, Kazuaki; Murai, Shinji; Sonoda, Noboru
Journal of Organic Chemistry, 1987 , vol. 52, p. 4864 - 4868
反应条件
sulfuric acid 5 h; Heating;
参考文献
Fleming, Ian; Patel, Shailesh K.; Urch, Christopher J.
Journal of the Chemical Society, Perkin Transactions 1: Organic and Bio-Organic Chemistry (1972-1999), 1989 , p. 115 - 124
参考文献
Revis, Anthony; Hilty, Terrence K.
Tetrahedron Letters, 1987 , vol. 28, # 41 p. 4809 - 4812
反应条件
hydrogenchloride; sec.-butyllithium 1.) THF, Et2O, pentane, -90 deg C, 3 h, 2.) THF, Et2O, pentane, 30 min; Yield given. Multistep reaction;
参考文献
Seyferth, Dietmar; Mammarella, Robert E.; Klein, Helmut A.
Journal of Organometallic Chemistry, 1980 , vol. 194, # 1 p. 1 - 8
反应条件
sec.-butyllithium 1.) THF, Et2O, pentane, -90 deg C, 3 h, 2.) THF, Et2O, pentane, 30 min; Yield given. Multistep reaction. Yields of byproduct given;
参考文献
Seyferth, Dietmar; Mammarella, Robert E.; Klein, Helmut A.
Journal of Organometallic Chemistry, 1980 , vol. 194, # 1 p. 1 - 8
参考文献
Petrow et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 2936;engl.Ausg.S.2896
参考文献
Petrow et al.
Zhurnal Obshchei Khimii, 1959 , vol. 29, p. 2936;engl.Ausg.S.2896
