in neat (no solvent) byproducts: Me3SiNCO, (Me3Si)2NH, (Me3Si)2O; mixt. of reagents at molar ratio of 1:1 (two-fold excess of (Bu3Sn)2O) heated from 80 to 170° and gradually evacuated from 760 to 3-5 mmHg over a period of 1 h; identified by elem. anal. and IR spectrum;
参考文献
Gordetsov; Kulagina; Zimina
Russian Journal of General Chemistry, 2000 , vol. 70, # 3 p. 409 - 412
