1,4-环己二酮双乙二醇二缩酮合成路线 （共 14 条）
反应条件
iodine in chloroform T=20°C; 2 h;
参考文献
Firouzabadi; Iranpoor; Hazarkhani
Journal of Organic Chemistry, 2001 , vol. 66, # 22 p. 7527 - 7529
反应条件
1: H2O / acetic acid; trifluoroacetic acid / 14 h / 45 °C 2: 88 percent / dimethylsulfoxide; benzene / 2 h / 25 °C 3: 1.) diisoamylborane, 2-methyl-2-butene, 2.) 30percent H2O2, 3N NaOH / 1.) 0 deg C, 3 h, 2.) -10 deg C -> RT, 30 min View Scheme
参考文献
Nicolaou; Magolda; Claremon
Journal of the American Chemical Society, 1980 , vol. 102, # 4 p. 1404 - 1409
反应条件
hydrogenchloride; palladium in water; acetic acid
参考文献
IMPERIAL CHEMICAL INDUSTRIES PLC
Patent: EP343798 A1, 1989 ;
反应条件
1: H2O / acetic acid; trifluoroacetic acid / 14 h / 45 °C
2: 88 percent / dimethylsulfoxide; benzene / 2 h / 25 °C
View Scheme
参考文献
Nicolaou; Magolda; Claremon
Journal of the American Chemical Society, 1980 , vol. 102, # 4 p. 1404 - 1409
