2-乙酰基-3-羟基-2-丁酸乙酯合成路线 (共 4 条)
反应条件
1: ethyl acetoacetate With tetrachloromethane; ethanol; magnesium in toluene 1 h; Heating; 2: acetyl chloride in tetrachloromethane; ethanol; toluene T=20°C; 1 h;
参考文献
Jung, Jae-Chul; Watkins, E.Blake; Avery, Mitchell A
Tetrahedron, 2002 , vol. 58, # 18 p. 3639 - 3646
反应条件
zinc(II) chloride in acetone Heating;
参考文献
Buechi,G.; Wuest,H.
Helvetica Chimica Acta, 1971 , vol. 54, p. 1767 - 1775
反应条件
hydrazine in ethanol T=20°C; 16 h;
参考文献
Jung, Jae-Chul; Watkins, E.Blake; Avery, Mitchell A
Tetrahedron, 2002 , vol. 58, # 18 p. 3639 - 3646
反应条件
hydrazine monohydrochloride in ethanol T=20°C; 16 h;
参考文献
Jung, Jae-Chul; Watkins, E.Blake; Avery, Mitchell A
Tetrahedron, 2002 , vol. 58, # 18 p. 3639 - 3646